Zoro used Haki pre-timeskip?

SSJ2

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No, imbuing is part of level 1 along with hardening.
 

SSJ2

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Because he was a swordsman.

Turning a blade black is a swordsman's equivalent of turning your arm/body black. It's basic level one Busoshoku. This can be combined with level 2 Busoshoku which Hyogoro showed:

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Zoro has never used this level of Haki to my knowledge.
 
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